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The Resource Essential practical NMR for organic chemistry, S.A. Richards and J.C. Hollerton

Essential practical NMR for organic chemistry, S.A. Richards and J.C. Hollerton

Label
Essential practical NMR for organic chemistry
Title
Essential practical NMR for organic chemistry
Statement of responsibility
S.A. Richards and J.C. Hollerton
Creator
Contributor
Subject
Language
eng
Summary
"This book describes the use of NMR spectroscopy for dealing with problems of small organic molecule structural elucidation. It features a significant amount of vital chemical shift and coupling information but more importantly, it presents sound principles for the selection of the techniques relevant to the solving of particular types of problem, whilst stressing the importance of extracting the maximum available information from the simple 1-D proton experiment and of using this to plan subsequent experiments. Proton NMR is covered in detail, with a description of the fundamentals of the technique, the instrumentation and the data that it provides before going on to discuss optimal solvent selection and sample preparation. This is followed by a detailed study of each of the important classes of protons, breaking the spectrum up into regions (exchangeables, aromatics, heterocyclics, alkenes etc.). This is followed by consideration of the phenomena that we know can leave chemists struggling; chiral centres, restricted rotation, anisotropy, accidental equivalence, non-first-order spectra etc. Having explained the potential pitfalls that await the unwary, the book then goes on to devote chapters to the chemical techniques and the most useful instrumental ones that can be employed to combat them. discussion is then presented on carbon-13 NMR, detailing its pros and cons and showing how it can be used in conjunction with proton NMR via the pivotal 2-D techniques (HSQC and HMBC) to yield vital structural information. Some of the more specialist techniques available are then discussed, i.e. flow NMR, solvent suppression, Magic Angle Spinning, etc. Other important nuclei are then discussed and useful data supplied. This is followed by a discussion of the neglected use of NMR as a tool for quantification and new techniques for this explained. The book then considers the safety aspects of NMR spectroscopy, reviewing NMR software for spectral prediction and data handling and concludes with a set of worked Q & As"--Provided by publisher
Member of
Cataloging source
DG1
http://library.link/vocab/creatorName
Richards, S. A
Dewey number
543/.66
Illustrations
illustrations
Index
index present
Language note
English
LC call number
QD96.P7
LC item number
R529 2011eb
Literary form
non fiction
Nature of contents
dictionaries
http://library.link/vocab/relatedWorkOrContributorDate
1959-
http://library.link/vocab/relatedWorkOrContributorName
Hollerton, J. C.
http://library.link/vocab/subjectName
  • Proton magnetic resonance spectroscopy
  • Nuclear magnetic resonance spectroscopy
  • Magnetic Resonance Spectroscopy
  • Protons
  • Nuclear Magnetic Resonance, Biomolecular
  • SCIENCE
  • Nuclear magnetic resonance spectroscopy
  • Proton magnetic resonance spectroscopy
Label
Essential practical NMR for organic chemistry, S.A. Richards and J.C. Hollerton
Instantiates
Publication
Bibliography note
Includes bibliographical references and index
Carrier category
online resource
Carrier category code
  • cr
Carrier MARC source
rdacarrier
Color
multicolored
Content category
text
Content type code
  • txt
Content type MARC source
rdacontent
Contents
Getting Started -- Preparing the Sample -- Spectrum Acquisition -- Processing -- Interpreting Your Spectrum -- Delving Deeper -- Further Elucidation Techniques : Part 1 -- Further Elucidation Techniques : Part 2 -- Carbon-13 NMR Spectroscopy -- Some of the Other Tools -- Some of the Other Nuclei -- Quantification -- Safety -- Software -- Problems
Control code
689995820
Dimensions
unknown
Extent
1 online resource (x, 216 pages)
Form of item
online
Isbn
9780470976395
Media category
computer
Media MARC source
rdamedia
Media type code
  • c
Other control number
  • 9786612884061
  • 10.1002/9780470976401
Other physical details
illustrations (some color)
http://library.link/vocab/ext/overdrive/overdriveId
10.1002/9780470976401
Specific material designation
remote
System control number
(OCoLC)689995820
Label
Essential practical NMR for organic chemistry, S.A. Richards and J.C. Hollerton
Publication
Bibliography note
Includes bibliographical references and index
Carrier category
online resource
Carrier category code
  • cr
Carrier MARC source
rdacarrier
Color
multicolored
Content category
text
Content type code
  • txt
Content type MARC source
rdacontent
Contents
Getting Started -- Preparing the Sample -- Spectrum Acquisition -- Processing -- Interpreting Your Spectrum -- Delving Deeper -- Further Elucidation Techniques : Part 1 -- Further Elucidation Techniques : Part 2 -- Carbon-13 NMR Spectroscopy -- Some of the Other Tools -- Some of the Other Nuclei -- Quantification -- Safety -- Software -- Problems
Control code
689995820
Dimensions
unknown
Extent
1 online resource (x, 216 pages)
Form of item
online
Isbn
9780470976395
Media category
computer
Media MARC source
rdamedia
Media type code
  • c
Other control number
  • 9786612884061
  • 10.1002/9780470976401
Other physical details
illustrations (some color)
http://library.link/vocab/ext/overdrive/overdriveId
10.1002/9780470976401
Specific material designation
remote
System control number
(OCoLC)689995820

Library Locations

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      400 West 14th Street, Rolla, MO, 65409, US
      37.955220 -91.772210
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